CIP Code: 40.0502 HEGIS Code: 1909 METROPOLITAN STATE COLLEGE OF DENVER Office of Academic Affairs REGULAR COURSE SYLLABUS SCHOOL: Letters, Arts, and Sciences DEPARTMENT: Chemistry SEMESTER(S) OFFERED: Fall, Spring, Summer PREFIX & COURSE NUMBER: CHE300 COURSE TITLE: Analytical Chemistry CREDIT HOURS: 3 ( 3 + 0 ) CONTACT HOURS: Lecture 45 Lab 0 Internship 0 Practicum 0 RESTRICTIONS (VARIABLE TOPICS COURSES): None PREREQUISITE(S): CHE 180, CHE 181, and CHE 185 COREQUISITE(S): CHE 301 to be taken concurrently CATALOG COURSE DESCRIPTION: A study of the fundamentals of analytical chemistry including principles of gravimetric, volumetric, potentiometric, and spectrophotometric analyses. REQUIRED READING MATERIALS (Title, Author, Publisher, Copyright Date): Analytical Chemistry; Skoog, D.A., Holler F.J., and West, D.M., 6th Ed; Holt, Rinehart Winston Publishing Company, 1994. SPECIFIC (MEASURABLE) STUDENT BEHAVIORAL LEARNING OBJECTIVES: Upon completion of this course the student should be able to: 1. Determine the solubility of precipitates. 2. Determine the conditions for maximum stability of precipitates. 3. Determine the conditions necessary for quantitative precipitation. 4. Compute the pH of solutions of strong acids, strong bases, weak acids, weak bases, polyprotic acids, poly basic compounds, and arbitrary mixtures of the above. 5. Compute theoretical titration curves for acids and bases of arbitrary types. 6. Choose indicators for acid-base titrations, precipitation titrations, complexation, and redox titrations. 7. Calculate cell potentials using the Nernst equation. 8. Calculate species concentrations in simple complexation reactions. 9. Calculate redox titration curves for oxidation-reduction titrations. 10. calculate theoretical titration curves in simple and multiple complexation reactions at various pH. 11. Choose optimum conditions for selective complexometric titration using masking agents and/or control of pH. 12. Finalize the Beer-Lampert Law to find E values and concentrations. 13. Choose optimum wave length values for analysis from an absorption curve. 14. Perform a calculation for multi-component spectrophotometric analysis. 15. Recognize and apply the limitation of applicability of the Beer-Lampert Law. 16. Explain the principles of operation of single beam and double beam spectrophotometers. OUTLINE OF COURSE CONTENT (Major Topics and Subtopics): I. Introduction II. Types of Analyses Statistics Applies to Analytical Chemistry III. Gravimetric Analysis Principles of the Methods solubility equilibria optimization of precipitation parameters practical examples IV. Volumetric Analysis equilibria in solution practical examples V. Potentiometry The Nernst equation and applications potentiometric cells potentiometric titrations VI. Spectrophotometry Beer-Lampert Law applications limitations instrumentation EVALUATION OF STUDENT PERFORMANCE: Students will be given periodic fifty minute examinations. These examinations will be supplemented by short quizzes. A final exam one hundred minutes long will terminate the course. The final grade determination will be based on the students performance on the examinations, quizzes, final exam, and the instructors evaluation. Copies retained by Dean and Department Chair Revised 9/94: Academic Affairs-Curriculum-Regular Course Syllabus (s:\wpform\acadaff\currculm\regsyl.wp)